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À propos de : Synthesis of the First Poly(pyrazolyl)borateComplex of Germanium(II): Solid StateStructure of [HB(3,5-Me2pz)3Ge]I·1/2CH2Cl2        

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  • Synthesis of the First Poly(pyrazolyl)borateComplex of Germanium(II): Solid StateStructure of [HB(3,5-Me2pz)3Ge]I·1/2CH2Cl2
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  • Thereaction of K[HB(3,5-Me2pz)3] andGeCl2(dioxane) in THF solution yields the ionic complex[HB(3,5-Me2pz)3Ge]Cl.Metathesis with NaI yields[HB(3,5-Me2pz)3Ge]I. The solidstate structure of[HB(3,5-Me2pz)3Ge]I·1/2CH2Cl2shows well-separated, three-coordinate, germanium-basedcations and iodide anions. The cation[HB(3,5-Me2pz)3Ge]+represents the first stable germanium poly(pyrazolyl)boratecomplex and the first poly(pyrazolyl)borate complex ofgermanium(II).
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