About: Radical Deoxygenation of Hydroxyl Groups via Phosphites

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Attributs	Valeurs
type	work Article
Is Part Of	http://hub.abes.fr/acs/periodical/jacsat/2004/volume_126/issue_41/w
Subject	Communication
Title	Radical Deoxygenation of Hydroxyl Groups via Phosphites
has manifestation of work	http://hub.abes.fr/acs/periodical/jacsat/2004/volume_126/issue_41/101021ja0462777/m/print http://hub.abes.fr/acs/periodical/jacsat/2004/volume_126/issue_41/101021ja0462777/m/web
related by	http://hub.abes.fr/acs/periodical/jacsat/2004/volume_126/issue_41/101021ja0462777/authorship/1 http://hub.abes.fr/acs/periodical/jacsat/2004/volume_126/issue_41/101021ja0462777/authorship/2
Author	Zhang Liming Koreeda Masato
Abstract	A highly efficient, two-step sequence method for the deoxygenation of hydroxyl groups has been developed. The method involves the preparation of the 2-(2-iodophenyl)ethyl methyl phosphite derivative of an alcohol using methyl dichlorophosphite and 2-(2-iodophenyl)ethanol. Treatment of the phosphite intermediate with (n-Bu)3SnH/AIBN in refluxing benzene cleanly produces the deoxygenation product of the original alcohol.
article type	rapid-communication
is part of this journal	Journal of the American Chemical Society

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