About: Synthesis of Thioglycoside-BasedUDP-Sugar Analogues

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Attributs	Valeurs
type	work Article
Is Part Of	http://hub.abes.fr/acs/periodical/joceah/2004/volume_69/issue_21/w
Subject	Note
Title	Synthesis of Thioglycoside-BasedUDP-Sugar Analogues
has manifestation of work	http://hub.abes.fr/acs/periodical/joceah/2004/volume_69/issue_21/101021jo049077m/m/web http://hub.abes.fr/acs/periodical/joceah/2004/volume_69/issue_21/101021jo049077m/m/print
related by	http://hub.abes.fr/acs/periodical/joceah/2004/volume_69/issue_21/101021jo049077m/authorship/2 http://hub.abes.fr/acs/periodical/joceah/2004/volume_69/issue_21/101021jo049077m/authorship/3 http://hub.abes.fr/acs/periodical/joceah/2004/volume_69/issue_21/101021jo049077m/authorship/1
Author	Schmidt Richard R. Stolz Florian Zhu Xiangming
Abstract	Arbuzov reaction of O-acetyl-protected glycosylthiomethyl chlorides with triethyl phosphite and thenphosphonate ethyl ester cleavage with trimethylsilyl bromide afforded glycosylthiomethyl phosphonates 13, 18, 22,and 26. These intermediates could be readily transformedinto the O-deprotected phosphonates 7−10 and into titlecompounds 1−4. Similarly, sulfonomethyl phosphonate moieties containing UDP-sugar analogues 5 and 6 were obtained.
article type	brief-report
is part of this journal	The Journal of Organic Chemistry

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