About: Simple, Rapid Procedure for the Synthesisof Chloromethyl Methyl Ether and OtherChloro Alkyl Ethers1

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Attributs	Valeurs
type	work Article
Is Part Of	http://hub.abes.fr/acs/periodical/joceah/2005/volume_70/issue_23/w
Subject	Note
Title	Simple, Rapid Procedure for the Synthesisof Chloromethyl Methyl Ether and OtherChloro Alkyl Ethers1
has manifestation of work	http://hub.abes.fr/acs/periodical/joceah/2005/volume_70/issue_23/101021jo051344g/m/web http://hub.abes.fr/acs/periodical/joceah/2005/volume_70/issue_23/101021jo051344g/m/print
related by	http://hub.abes.fr/acs/periodical/joceah/2005/volume_70/issue_23/101021jo051344g/authorship/2 http://hub.abes.fr/acs/periodical/joceah/2005/volume_70/issue_23/101021jo051344g/authorship/1
Author	Belecki Katherine Berliner Martin A.
Abstract	Zinc(II) salts catalyze the reaction between acetals and acidhalides to provide haloalkyl ethers in near-quantitativeyield. Reactions from millimole to mole scale are typicallycomplete in 1−4 h with 0.01 mol % catalyst. The solutionsof haloalkyl ethers thus obtained can be utilized directly inreactions in which the presence of the ester byproduct doesnot interfere. Excess haloalkyl ether is destroyed on workup,thereby minimizing exposure to this class of carcinogeniccompounds.
article type	brief-report
is part of this journal	The Journal of Organic Chemistry

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