About: Ruthenium-Catalyzed Mild C−HOxyfunctionalization of Cyclic Steroidal Ethers1

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Attributs	Valeurs
type	work Article
Is Part Of	http://hub.abes.fr/acs/periodical/joceah/2007/volume_72/issue_15/w
Subject	Note
Title	Ruthenium-Catalyzed Mild C−HOxyfunctionalization of Cyclic Steroidal Ethers1
has manifestation of work	http://hub.abes.fr/acs/periodical/joceah/2007/volume_72/issue_15/101021jo070382s/m/print http://hub.abes.fr/acs/periodical/joceah/2007/volume_72/issue_15/101021jo070382s/m/web
related by	http://hub.abes.fr/acs/periodical/joceah/2007/volume_72/issue_15/101021jo070382s/authorship/1 http://hub.abes.fr/acs/periodical/joceah/2007/volume_72/issue_15/101021jo070382s/authorship/2 http://hub.abes.fr/acs/periodical/joceah/2007/volume_72/issue_15/101021jo070382s/authorship/3
Author	Fuchs Philip L. Lee Jong Seok Cao Hui
Abstract	Ruthenium-catalyzed site-specific C−H oxyfunctionalizationof steroidal ethers with periodate or bromate as terminaloxidants in phosphate buffer provided the acid-sensitive C-16hydroxy compounds in high yields. Phosphate buffer (pH7.5) significantly inhibits formation of unwanted sideproducts generated under more acidic reaction conditions.A key example is demonstrated at the 100 g scale.
article type	brief-report
is part of this journal	The Journal of Organic Chemistry

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